Speciicaions autopore iv 9500 series low pressure measurement 0 to 50 psia 345 kpa pore diameter range 360 to 3. Particlesize distribution an overview sciencedirect. Autopore iii, micromeritics, norcross, ga, usa following astm d4404 43 standard procedure. The instrument also comes with improved safety features and provides new data reduction and reporting options which offer more data regarding fluid. In addition, aged samples were washed in distilled water during one week after the. The mercury porosimetry analysis technique is based on the intrusion of mercury into a porous structure under stringently controlled pressures. Pore size distribution of granulation and tablets was determined by mercury intrusion porosimetry mip, autopore iii, micromeritics, norcross, ga, united states. Characterization of the catalysts surface areas of the supports were determined from desorption isotherms of nitrogen adsorbed at. Micromeritics micromeritics is the science and technology of small particles. Autopore iv 9500 series measures sample porosity laboratory. Micromeritics, usa, was used to measure skeletal density. The sedigraph iii plus from micromeritics is designed to determine particle size using the proven sedigraph technique with advanced instrumentation features to provide superior accuracy, repeatability, and reproducibility. Micromeritics autopore iv 9500 series characterizes a materials porosity by applying various levels of pressure to a sample immersed in mercury.
Mercury porosimetry of certified silicaalumina reference. Feb 02, 2018 micromeritics, introduction of micromeritics, applications of micromeritics, particle size, particle size in pharmaceutical dimensions. Using a gas displacement technique to measure volume, the accupyc ii 40 completes most sample analyses in less than three minutes. Sep 07, 2015 micromeritics micromeritics is the science and technology of small particles. The autopore iv seriesuses mercury intrusion and extrusion to. Micromeritics is powders engineering specialized magazine publication annual from 1957. Comparison of wickekallenbach and grahams diffusion cells. The particles of pharmaceutical emulsion and suspension and the fines of powder fall in the range of the optical microscope.
The autopore v series porosimeters from micromeritics use the mercury porosimetry analysis method, in which mercury is introduced into a porous structure under closely monitored pressures. The asap 2020 can obtain highquality data for research and quality control applications and is designed to provide. Countercurrent gas diffusion measurements on a series of porous solids covering a broad range of pore sizes mean pore radii between 78nm and 10. Autopore v series mercury porosimeters pharmaceutical online. Tips in measurement, pore structure parameter acquisition and application. The porosity of the membrane was measured by mercury intrusion porosimeter for meso and macropore analysis autopore iii, micromeritics usa, din 663 at bam federal institute for materials. But, coal utilization has the problem that emission amount of carbon dioxide. You can enter values for the advancing contact angle intrusion. Autopore iv series mercury porosimeter 9500 and 9510. The flowsorb iii 23052310 from micromeritics provides singlepoint surface area measurements with exceptional speed, accuracy and reliability. Besides offering speed, accuracy, and a wide measurement range, mercury porosimetry permits you to calculate numerous sample properties. Our distinguished faculty are highly recognized experts in materials characterization, with. Micromeritics sedigraph iii plus particle size analyzer. The pore size distribution was determined by mercury porosimetry using an autopore iii micromeritics.
Micromeritics study in different formulation colloidal dispersion are characterized by particles that are too small to be seen in the ordinary. On the modelling of algal biofouling growth on nanotio2. Micromeritics pycnometers are used worldwide to measure volume and determine material density of powders and solids. Knowledge and control of the size and the size range of particles are of significant importance in pharmacy.
The autopore iv 9500 series of mercury porosimeters from micromeritics enable the user to calculate numerous sample properties. Certified silicaalumina reference material micromeritics pn0041682200 0201 the samples were analysed using a micromeritics autopore iii 9420 mercury porosimeter which covers the pore diameter range from approximately 360 to 0. These include pore size distributions, total pore volume, total pore surface area, median pore diameter and sample densities bulk and skeletal. The unit of particle size most frequently used in micromeritics is micrometer, also called as a micron. For determining the exact contact angle, micromeritics offers the contact anglometer model 1501. Micromeritics has recently developed a new method of verifying that. Our distinguished faculty are highly recognized experts in materials characterization, with many years of commercial and academic research experience in this field. May 07, 2002 the flowsorb iii 23052310 from micromeritics provides singlepoint surface area measurements with exceptional speed, accuracy and reliability. Autopore iv series porosimeters pharmaceutical online. The accupyc ii 40 series pycnometers are fast, fully automatic analyzers that provide highspeed, highprecision volume measurements and density calculations on a wide variety of powders, solids, and slurries. To request a quote or additional product information, visit micromeritics web site at. The accupyc ii 40 series pycnometers are fast, fully automatic analyzers that provide highspeed, highprecision volume measurements and density calculations on a wide variety of powders, solids, and. The pressure required to intrude mercury into the samples.
Micromeritics autopore iv 9500 series characterise a materials porosity by applying. The knowledge and control of the size of particles is of importance in pharmacy and materials science. Ive only been employed by micromeritics for a little over 3 weeks but my experience has been inconceivable. Micromeritics, auto pore iii, mercury intrusion porosimeter. Certified silicaalumina reference material micromeritics pn0041682200 0201 the samples were analysed using a micromeritics autopore iii 9420 mercury porosimeter which covers the pore. Besides offering speed, accuracy, and a wide measurement. Introduction to chemical adsorption analytical techniques. Autopore iv advantages ability to measure pore diameters from 0. The autopore v series porosimeters are based on the mercury porosimetry analysis method. Introduction the science and technology of small particles was given by the name micromeritics by.
The mercury porosimetry analysis technique is based on. Particlesize distribution an overview sciencedirect topics. Micromeritics instrument corporation 38in sample tube manufacturer. Knowledge and control of the size and the size range of particles are of significant importance in pharmacy because the size and surface area of a particle related to the physical, chemical and pharmacologic properties of a drug. At first i was a bit nervous entering the position because it was different from the tasks ive done in the past. The annual conference of china scientific instruments accsi recently recognized micromeritics autopore v mercury porosimeter as one of the leading new instruments introduced to the china marketplace in 2014.
Coal is expected stable supply for the future because minable reserves of coal are more abundant than that of other fossil fuel. Mercury intrusion porosimetry mip is a powerful technique utilized for the evaluation of porosity, pore size. The open porosity p was calculated by the relation p 1. A fraction of the tablet or a granulation sample of the particle size fraction passing through 60mesh screen and retained on 100mesh screen was used for the porosity determination. Mercury porosimetry is a fast and precise technique for porosity characterization with a broad measurement range, suitable for a wide range of sample types. Micromeritics learning center mlc courses are presented in a professional, class room and laboratory setting. Micropore analysis can be performed on the tristar ii and gemini vii with the use of co2. Understanding the physical characteristics in particle size is important for various elements of research and development, quality control and assurance as well as production in the powder. At first i was a bit nervous entering the position because it was different from the tasks. It is thus the study of the fundamental and derived properties of individual as well as a collection of particles. Pore size distributions were obtained from mercury porosimeter working in the range 0. This is called mercury porosimetry, or often, mercury intrusion.
The pressure required to intrude mercury into the samples pores is inversely proportional to the size of the pores. The annual best new scientific instruments awards are presided over by 60 senior experts. Our latest offering, the autopore iv series of mercury porosimeters, provides the same highquality analysis data as expected from other micromeritics products and, in addition, comes with enhanced data reduction and reporting packages, faster pressure ramp rates, a more flexible and controllable vacuum system, and a redesign of both the low. The term micromeritics was given to the science and technology of small particles by j. The fourth industrial revolution is now dawning, and like the previous industrial revolutions, industry is going to have to adapt to the new technologies if it is to remain competitive and meet the expectations of its customers in terms of delivery and product quality. Mip measurements were performed with a micromeritics autopore. Mercury intrusion porosimetry in concrete technology. The flowsorb iii measures surface area using the flowing gas method, which involves the continuous flow of an adsorptive and inert gas mixture over the sample at atmospheric pressure. Micromeritics autopore iv porosimeters 9500 series. We offer the information of the technique in conjunction with powders and the engineering basics, application and the latest trend and serve in order to contribute to development of the powders engineering.
Analysis of the transient response and durability characteristics of a proton exchange membrane fuel cell with different microporous layer penetration thicknesses cho, junhyun park, jaeman oh. The autopore iv software allows you to enter the precise angle of. Improvements to a classic technique sedigraph iii plus particle size analyzer proven technique and reliability for over four decades, the micromeritics sedigraph has remained the standard instrument for particle size analysis in many laboratories throughout the world. These articles have been written by micromeritics research and applications scientists. An instant multiresponsive porous polymer actuator driven. Coatings 2018, 8, 54 2 of smooth surfaces 22, even if algal growth is not inhibit on the substrate,2325 and to facilitate its removal on some substrates through the formation of a super. The autopore iv generates tabular and graphical reports of percentage pore volume vs. The porosity of the membrane was measured by mercury intrusion porosimeter for meso and macropore analysis autopore iii, micromeritics usa, din 663 at bam federal institute for. Autopore v series mercury porosimeters from micromeritics are capable of determining a wider pore size distribution more quickly and precisely, giving it a great advantage over other methods. Pdf mercury intrusion porosimetry in concrete technology. Micromeritics instrument corporation 2366170300 this item has a minimum order quantity of 4 per supplier requirements. All data were obtained using a micromeritics autopore high pressure mercury. Micromeritics, introduction of micromeritics, applications of micromeritics, particle size, particle size in pharmaceutical dimensions.
Implication and evaluation of micromeritics in formulation 2. The annual conference of china scientific instruments accsi recently recognized micromeritics autopore v mercury porosimeter as one of the leading new. Introduction the science and technology of small particles was given by the name micromeritics by dalla valle micromeritics is the science and technology of small particles. It is thus the study of the fundamental and derived properties of individual as well as. The autopore features several levels of mechanical and electromechanical safety devices. Autopore application notes, scientific articles and. An instant multiresponsive porous polymer actuator driven by.
Micromeritics tristar ii plus surface area and porosity analyser. The ability to locate several research papers in which data from the same micromeritics product is published provides objective reassurance of. Micromeritics study in different formulation colloidal dispersion are characterized by particles that are too small to be seen in the ordinary microscope. The flowsorb iii 23052310 provides singlepoint and multipoint bet surface area measurements with speed, accuracy and reliability.
Micromeritics instrument corporation 38in sample tube 3. Our latest offering, the autopore iv series of mercury porosimeters, provides the same highquality analysis data as expected from other micromeritics products and, in addition, comes with enhanced. Comparison of wickekallenbach and grahams diffusion. Micromeritics instrument corporation 38in sample tube 38in.
988 395 476 441 487 50 779 393 462 553 167 1474 230 798 125 1379 150 1306 506 312 69 136 240 202 866 993 1230 95 1463 304 184 1073 36 3 463 1058